wet strip process

**Wet Strip Process** is the **chemical removal of photoresist and process residues using liquid solvents or oxidizing chemistries** — complementary to plasma ashing, applied where plasma damage to sensitive underlying layers must be avoided. **Wet Strip Chemistries** **Sulfuric Acid + Hydrogen Peroxide (SPM / Piranha)**: - H2SO4:H2O2 (4:1), 120–140°C. - Extremely aggressive organic removal — destroys resist in seconds. - Generates heat (exothermic) — "piranha" solution. - Used before gate oxidation, after implant strip. - Leaves surface clean of organic material but may require additional metal clean. **NMP (N-Methyl-2-Pyrrolidone) / EKC**: - Polar aprotic solvents with amine additives. - Swell and dissolve unexposed or lightly-exposed resist. - Used for post-etch residue removal (organic + some inorganic). - Temperature: 70–90°C, immersion or spray. - Cu compatible: Does not corrode copper. **ACT / EKC 265**: - Hydroxylamine + solvent + corrosion inhibitor. - Removes post-metal-etch residue — works with Cu, Al, TiN. - Low pH, compatible with most metals. **DS-20 (Dilute H2SO4)**: - Dilute sulfuric acid strip — gentler than piranha. - Strips implanted resist without leaving metal contamination. **When to Use Wet vs. Plasma Strip** | Situation | Preferred Strip | |-----------|----------------| | Post-implant resist | Plasma ash first, then SPM | | Hardened crust resist | Plasma ash first | | Cu BEOL post-etch | Wet (EKC/ACT) — no O2 plasma on Cu | | Sensitive III-V surface | Wet only | | Organic residue on oxide | Plasma ash | **Process Integration** - Most flows use two-step: O2 plasma ash bulk + wet strip final clean. - Single-step wet: Reserved for Cu-incompatible-plasma applications. Wet strip process selection is **a critical integration decision** — choosing the wrong chemistry damages underlying films or leaves unacceptable residues that cause device failures or contamination of subsequent process steps.

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